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Skunks are nocturnal. Few hours before sundown, crumple newpapers and block the hole with it.
After the sun sets, check the hole every 15 mins and see if the newspaper has moved. If the newspaper has moved, here is your chance to fill the hole/block it with a big rock.
Skunks only know how to dig under things, they don't know how to jump over things.
If the skunk digs his way back under your shed, then fox urine might be the 2nd option. (seriously, no joke)
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